1-Bromotetradecane Typical Properties
Item |
Method of Analysis |
Standard |
Result |
appearance |
visual inspection |
Colorless transparent liquid |
Colorless transparent liquid |
Purity |
gas chromatography |
≥99.0% |
99.36% |
moisture |
– |
<0.05% |
0.038% |
1-Bromotetradecane Usage
Used in organic synthesis, can be used in the synthesis of medicine and other fine chemicals.
production method
Derived from tetradecanol by bromination.
- Add myristyl alcohol to the reaction pot, add sulfuric acid dropwise with stirring, and continue stirring for half an hour after the addition.
- Then add hydrobromic acid, heat to 99-101 ℃, and react for 8h. Cool to 30 ° C, stop stirring, leave for 12h, separate the upper oily substance, and adjust the pH to 8 with 10% sodium carbonate solution.
- Separate the water layer, and wash the oil twice with an equal volume of 50% ethanol. Add the washed oil to sodium carbonate, stir intermittently, and dry for 24 hours. Filter to get the finished product.
1-Bromotetradecane Packing
25kgs/drum
1-Bromotetradecane Storage
1-Bromotetradecane should be stored in a closed system, and be kept in a dry dark place without any light exposure. The shelf life is two years in original, unopened containers.