5-Nitroisophthalic acid CAS 618-88-2

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5-Nitroisophthalic acid CAS 618-88-2

Products Name


Hot Sale factory provide 5-Nitroisophthalic acid 618-88-2 with best price  

Products Description

MF:C8H5NO6
EINECS No.:210-568-3
Purity:99%
Type:Pharmaceutical Intermediates
Appearance:white powder
Application:Pharmaceutical Intermediates Inquiry Now

5-Nitroisophthalic acid Typical Properties

Melting point 259-261 °C(lit.)
Boiling point 350.79°C (rough estimate)
density 1.6342 (rough estimate)
refractive index 1.5282 (estimate)
Fp 120°C
Water Solubility Soluble in water.1.5 g/L at 20°C
BRN 1976587
CAS DataBase Reference 618-88-2(CAS DataBase Reference)
EPA Substance Registry System 1,3-Benzenedicarboxylic acid, 5-nitro-(618-88-2)

5-Nitroisophthalic acid Usage

1.Used as an intermediate in medicines, pesticides, dyes and pigments

2.Used as an intermediate in the diagnosis of new diaphane (X-ray contrast agent) and as an intermediate in the dispersion of dyes

3.An important intermediate for dispersing dyes. 5-nitroisophthalic acid is also the intermediate of the new diphthimide.

5-Nitroisophthalic acid Packaging and Shipping

Packaging:1kg or 5kgs/Aluminium bag,
25kgs/drum,
25 tons/20ft,Or it’s according to customers’ option

Shipping:It can be according to the customer’s request

5-Nitroisophthalic acid Storage

normal temperature preservation

Preparation method of 5-aminoisophthalic acid

(1) The nickel foam with a pore diameter of 0.2mm, a pore density of 110PPI and a porosity of ≥95% is pretreated with acetone, ethanol and distilled water ultrasonically, then dried in a vacuum, and placed in a tube furnace. The temperature was raised to 600°C and reacted with acetylene gas for 1 hour. After the reaction was completed, the temperature was lowered to room temperature in an argon atmosphere to obtain a foamed nickel/carbon nanotube magnetic catalyst. Among them, the foamed nickel/carbon nanotube magnetic catalyst was carbon nanotube. The content of the tube is 0.5% by weight.

(2) Add 5-nitro-isotitanic acid to water to fully dissolve it, transfer it to the reactor, add ammonia to adjust the pH of the system to 9, pass in 25mL/min of hydrogen, add foamed nickel/carbon nanotube magnetic catalyst, React at a constant temperature of 90°C for 100 minutes to obtain a 5-amino-isophthalic acid solution.

(3) After the 5-amino-isophthalic acid solution is recovered with a magnet catalyst, the mother liquor is recovered by filtration, acidified by adding hydrochloric acid, recrystallized at room temperature, and dried to obtain 5-amino-isophthalic acid.